2D Experiment Setup Steps

The following applies to all 1H-detected, 2D experiment setup unless otherwise instructed.

Step 1: Load sample, lock and shim as usual.

Step 2: Set 1H spectral width in direct detect dimension


Step 3: Use the selected 1H window size and set up 2D experiment

Step 4: Start experiment(s)


To stop an experiment, depending on which experiment to be stopped, do the following:


For all 2D (or any arrayed experiment), watch for ADC or receiver overflow immediately after the start of data collection.

H. Zhou Updated 04/2012