1D H1 and C13 Detection

H1 detection is the most basic experiment a user should be familiar with before attempting other experiments. On all instruments (except Bruker NMR800) the in-house initialization script init1h sets default H1 detection parameters. The following instructions are detailed during training, and are listed only briefly here.

Sample volume:

H1 detection steps

C13 detection steps (preferably on NMR500 and NMR600 where the X-channel is tuned to C13 at all time)

This experiment is a basic C13 detection experiment with H1→C13 NOE.

H. Zhou updated Aug 2011